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Article
Amide Synthesis through Selective Partial Hydrolysis of Nitriles in Alkaline Media
Author(s)
Raymundo Yáñez-Alarid, Elvira Santos-Santos and Eva F. Lejarazo-Gómez
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DOI:10.17265/1934-7375/2020.02.003
Affiliation(s)
Department of Organic Chemistry, Faculty of Chemistry, Postgraduate Studies Units, Circuito Exterior S/N, Ciudad Universitaria, CP 04510, Coyoacán, Mexico City, Mexico
ABSTRACT
Amides were obtained through partial hydrolysis
of nitriles, using two different energy sources, traditional heating with
solvent reflux and
ultrasound. The reaction was performed at micro and semi-micro scales and at
different reaction time with both energy sources.
Yield was determined through gas chromatography, in the case of micro-scale and
weight loss in the case of semi-micro scale.
KEYWORDS
Amide, hydrolysis of nitriles.
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