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Article
Author(s)
M. Sager
Full-Text PDF XML 7916 Views
DOI:10.17265/2159-5828/2019.02.007
Affiliation(s)
Austrian Agency for Health and Food Safety (AGES), Institute for Food Safety, Vienna, Austria
ABSTRACT
For determination of
iodine, dissolution or oxidation of an organic matrix by acid K-chlorate in
dilute nitric acid to obtain non-volatile iodate immediately, is a method of
choice. Optical emission spectroscopy is usually sensitive enough to control
iodized table salt. Spectral interference by P upon the most sensitive
I-emission line, e.g. in mineral feeds and marine algae, was overcome by
co-precipitation of P with Al- or Fe hydroxide, leaving iodate (and also
borate) in solution. After addition of Al or Fe nitrate or sulfate, ammonia was
added to reach pH 8.8,
and the resulting precipitate separated by cetrifugation and decantation.
Al-hydroxide was more efficient, and its precipitation was facilitated by
adding 10-30 mg of a natural clay to 5 mL sample. Correct results with
materials from former ring tests were obtained down to 15 mg/kg by an ICP 20
years of age.
KEYWORDS
Iodine, marine algae, feed premixes, ICP-OES.
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