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Rapid Microwave-accelerated Multi-step Synthesis of 2,6-di(naphthalene Thioureido Carbamino)Pyridine
Hairui Zhang and Guofu Zhang
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DOI:10.17265/1934-7375/2017.02.007
A rapid and simple procedure for synthesis of 2,6-di(naphthalene thioureido carbamino)pyridine fluorescine anion acceptor by the reaction between pyridine-2,6-dicarbohydrazide obtained from 2,6-dimethylpyridine after three-step reaction and 1-naphthyl isothiocyanate is described, and all reactions could be carried out under microwave heating condition.
2,6-di(naphthalene thioureido carbamino)pyridine, pyridine-2,6-dicarboxylic acid, dimethyl 2,6-pyridinedi- carboxylate, pyridine-2,6-dicarbohydrazide, microwave irradiation
[1] Wei, L., Wu, Y., Wang, F., Meng, L., and He, Y. 2003. “Fluorescent Receptor Containing Diaminothiourea Branches Synthesis and Anion Recognition.” Wuhan Univ. (Nat. Sci. Ed.) 49 (6): 709-12.
[2] Beer, P., and Gale, P. J. 2001. “Anion Recognition and Sensing: The State of the Art and Future Perspectives.” Angew. Chem. Int. Ed. Engl. 40: 486-516.
[3] Zhang, G., Zhang, H., Ye,, H., and Zhang, Q. 2011. “The Microwave Synthesis of 2,6-pyridine Dicarboxylic Hydrazine.” Journal of chemistry and Chemical Engineering 5 (11): 1041-5.
[4] Zhang, G., Zhang, Q., Zhang, H., Bai, L., Ye, H., and Liu, L. 2010. “The Synthesis of Pyridine 2,6-dicarboxylic Acid Using Microwave Irradiation.” Journal of Chemistry and Chemical Engineering 4 (11): 60-4.
[5] Zhang, G., Zhang, Q., Ye, H., Liu, L., and Zang, L. 2010. “Synthesis of 2,6-pyridine Dimethyl Formate under Microwave Irradiation.” Journal of Chemistry and Chemical Engineering 5 (3): 255-8.